Laser-Induced Graphene Oxide on Polyimide Sheet: The Effect of Current Regulation on the Laser Power Stability
DOI:
https://doi.org/10.26740/jpfa.v14n1.p100-112Keywords:
laser diode, stability, fluctuation, polyimide, laser-induced graphene oxideAbstract
Graphene oxide is a two-dimensional substance that shares the same structure as graphene and can be produced using several methods. The difficulty for green technology lies in developing a cost-effective and efficient method to produce graphene and graphene oxide without relying on chemical processes. A highly sustainable technology involves the use of a laser diode, which is both cost-effective and environmentally friendly. This technique produces a material known as laser-induced graphene/graphene oxide (LIG/LIGO). From a commercial standpoint, the laser diode is typically purchased without an electronic stabilizer component. Nevertheless, laser stability is crucial for the production process of LIG/LIGO. The objective of our study is to examine the impact of laser current management on the production of graphene on a polyimide (PI) sheet utilizing a 450 nm diode laser. The laser controller we utilize is the National Instruments (NI) PXIe-1085 device. The optical power of the laser diode was measured between 0.21 and 0.79 W. After the laser current was stabilized, the power slightly shifted, ranging from 0.18 to 0.86 W. Both experiments were conducted with a current range of 0.3 to 1 A. Before regulation, the laser diode experiences current fluctuations in the range of around 0.01 to 0.03 A. The study findings highlight the significance of laser current management in manufacturing LIG/LIGO by ensuring a consistent and precise laser power output, hence minimizing flaws in the final product. However, the analysis reveals that graphene oxide is the predominant yield in this characterization. This fact is caused by the presence of a graphene layer not exposed to the surface during measurement. This approach provides several benefits, such as the capacity to produce graphene/GO in a targeted, non-chemical, and fast manner, as well as its potential for diverse applications.
References
Murthy HCA, Ghotekar S, Vinay Kumar B, and Roy A. Graphene: A Multifunctional Nanomaterial with Versatile Applications. Advances in Materials Science and Engineering. 2021; 2021(1): 2418149. DOI: https://doi.org/10.1155/2021/2418149.
Kulyk B, Silva BFR, Carvalho AF, Silvestre S, Fernandes AJS, Martins R, et al. Laser-Induced Graphene from Paper for Mechanical Sensing. ACS Applied Materials and Interfaces. 2021; 13(8): 10210-10221. DOI: https://doi.org/10.1021/acsami.0c20270.
Winingsih PH. Rancang Bangun Laser Untuk Pembelajaran Optika Dalam Menentukan Indeks Bias Dan Difraksi Kisi. Science Tech: Jurnal Ilmu Pengetahuan Dan Teknologi. 2015; 1(1): 77–82. DOI: https://doi.org/10.30738/jst.v1i1.482.
Yan Y, Zheng Y, Sun H, and Duan J. Review of Issues and Solutions in High-Power Semiconductor Laser Packaging Technology. Frontiers in Physics. 2021; 9: 1–16. DOI: https://doi.org/10.3389/fphy.2021.669591.
Hasanah N. Analisis Penggunaan Cahaya Laser Untuk Menentukan Indeks Bias Kaca. Jurnal Sains dan Teknologi. 2022; 12(1): 28–33.
Michalik M, Szymańczyk J, Stajnke M, Ochrymiuk T, and Cenian A. Medical Applications of Diode Lasers: Pulsed Versus Continuous Wave (cw) Regime. Micromachines. 2021; 12(6): 1-15. DOI: https://doi.org/10.3390/mi12060710.
Sholahuddin. Studi Pembuatan Laser Induced Graphene pada Lembaran Polyimide dengan Laser Dioda 450 nm. Undergraduate Thesis. Unpublished. Jakarta: UIN Syarif Hidayatullah Jakarta; 2023.
Seifert F. Power Stabilization of High Power Lasers for Second Generation Gravitational Wave Detectors. PhD Thesis. Unpublished. Germany: Leibniz University Hannover; 2010.
Yu H, Gai M, Liu L, Chen F, Bian J, and Huang Y. Laser-Induced Direct Graphene Patterning: from Formation Mechanism to Flexible Applications. Soft Science. 2023; 3(4): 1–33. DOI: https://doi.org/10.20517/ss.2022.26.
Jeong SY, Ma YW, Lee JU, Je GJ, and Shin BS. Flexible and Highly Sensitive Strain Sensor Based on Laser-Induced Graphene Pattern Fabricated by 355 nm Pulsed Laser. Sensors. 2019; 19(22): 4867. DOI: https://doi.org/10.3390/s19224867.
Sartanavicius A, Zemgulyte J, Ragulis P, Ratautas K, and Trusovas R. Laser-Induced Graphene in Polyimide for Antenna Applications. Crystals. 2023; 13(7): 1003. DOI: https://doi.org/10.3390/cryst13071003.
Velasco A, Ryu YK, Hamada A, de Andrés A, Calle F, and Martinez J. Laser-Induced Graphene Microsupercapacitors: Structure, Quality, and Performance. Nanomaterials. 2023; 13(5): 788. DOI: https://doi.org/10.3390/nano13050788.
Romero FJ, et al. In-depth Study of Laser Diode Ablation of Kapton Polyimide for Flexible Conductive Substrates. Nanomaterials. 2018; 8(7): 517. DOI: https://doi.org/10.3390/nano8070517.
Stanford MG, Zhang C, Fowlkes JD, Hoffman A, Ivanov IN, Rack PD, et al. High-Resolution Laser-Induced Graphene: Flexible Electronics Beyond the Visible Limit. ACS Applied Materials and Interfaces. 2020; 12(9): 10902–10907. DOI: https://doi.org/10.1021/acsami.0c01377.
Li G. Direct Laser Writing of Graphene Electrodes. Journal of Applied Physics. 2020; 127(1): 010901. DOI: https://doi.org/10.1063/1.5120056.
Kothuru A and Goel S. Leveraging 3-D Printer with 2.8-W Blue Laser Diode to Form Laser-Induced Graphene for Microfluidic Fuel Cell and Electrochemical Sensor. IEEE Transactions on Electron Devices. 2022; 69(3): 1333–1340. DOI: https://doi.org/10.1109/TED.2022.3140707.
Avinash K and Patolsky F. Laser-Induced Graphene Structures: From Synthesis and Applications to Future Prospects. Materials Today. 2023; 70: 104–136. DOI: https://doi.org/10.1016/j.mattod.2023.10.009.
Cheng L, Guo W, Cao X, Dou Y, Huang L, Song Y, et al. Laser-Induced Graphene for Environmental Applications: Progress and Opportunities. Materials Chemistry Frontiers. 2021; 5(13): 4874–4891. DOI: https://doi.org/10.1039/D1QM00437A.
National Instruments Corp. Cascading the Outputs of the NI PXI-4130 Source Measure Units. Available from: https://www.ni.com/en/support/documentation/supplemental/12/cascading-the-outputs-of-the-ni-pxi-4130-source-measure-units.html [accessed 8 January 2024]
Ren M, Zhang J, and Tour JM. Laser-Induced Graphene Synthesis of Co3O4 in Graphene for Oxygen Electrocatalysis and Metal-air Batteries. Carbon. 2018; 139: 880–887. DOI: https://doi.org/10.1016/j.carbon.2018.07.051.
Tricot F, Phung DH, Lours M, Guérandel S, and De Clercq E. Power Stabilization of A Diode Laser with an Acousto-optic Modulator. Review of Scientific Instruments. 2018; 89(11): 113112. DOI: https://doi.org/10.1063/1.5046852.
Abedin KM, Al Jabri AR, and Mujibur Rahman SM. Power Stability of Different Lasers and its Effect on the Outcome of Phase-stepping Shearography Experiments. Results in Optics. 2023; 12: 100490. DOI: https://doi.org/10.1016/j.rio.2023.100490.
Adya A K and Canetta E. Nanotechnology and Its Applications to Animal Biotechnology. In Ashish S. Verma, Anchal Singh, Animal Biotechnology. Massachusetts: Academic Press; 2014: 247–263. DOI: https://doi.org/10.1016/B978-0-12-416002-6.00014-6.
Yoon H, Kim BH, Kwon SH, Kim DW, and Yoon YJ. Polyimide Photodevice without A Substrate by Electron-beam Irradiation. Applied Surface Science. 2021; 570: 151–185. DOI: https://doi.org/10.1016/j.apsusc.2021.151185.
Mahmood F, Zhang C, Xie Y, Stalla D, Lin J, and Wan C. Transforming Lignin Into Porous Graphene Via Direct Laser Writing for Solid-State Supercapacitors. RSC Advances. 2019; 9(39): 22713–22720. DOI: https://doi.org/10.1039/c9ra04073k.
Martins L, Kulyk B, Theodosiou A, Ioannou A, Moreirinha C, Kalli K, et al. Laser-Induced Graphene from Commercial Polyimide Coated Optical Fibers for Sensor Development. Optic and Laser Technology. 2023; 160: 109047. DOI: https://doi.org/10.1016/j.optlastec.2022.109047.
Guo Y, Zhang C, Chen Y, and Nie Z. Research Progress on the Preparation and Application of Laser-Induced Graphene Technology. Nanomaterials. 2022; 12(2): 23–36. DOI: https://doi.org/10.3390/nano12142336.
Wall M. The Raman Spectroscopy of Graphene and the Determination of Layer Thickness. Madison: Thermo Scientific; 2022. Available from: https://tools.thermofisher.com/content/sfs/brochures/AN52252_E+1111+LayerThkns_H_1.pdf.
Li Y, Luong DX, Zhang J, Tarkunde YR, Kittrell C, Sargunaraj F, et al. Laser-Induced Graphene in Controlled Atmospheres: From Superhydrophilic to Superhydrophobic Surfaces. Advanced Materials. 2017; 29(27): 1700496. DOI: https://doi.org/10.1002/adma.201700496.
Liu M, Wu JN, and Cheng HY. Effects of Laser Processing Parameters On Properties Of Laser-Induced Graphene by Irradiating CO2 Laser On Polyimide. Science China Technological Sciences. 2022; 65(1): 41–52. DOI: https://doi.org/10.1007/s11431-021-1918-8.
Mahmood F, Mahmood F, Zhang H, Lin J, and Wan C. Laser-Induced Graphene Derived from Kraft Lignin for Flexible Supercapacitors. ACS Omega. 2020; 5(24): 14611–14618. DOI: https://doi.org/10.1021/acsomega.0c01293.
An JW, Hyeong SK, Kim KM, Lee HR, Park J won, Kim TW, et al. Facile Synthesis of Laser‑Induced Graphene Oxide and its Humidity Sensing Properties. Carbon Letters. 2024; 34: 1173–1185. DOI: https://doi.org/10.1007/s42823-023-00672-3.
Hong S, Kim J, Jung S, Lee J, and Shin BS. Surface Morphological Growth Characteristics of Laser-Induced Graphene with UV Pulsed Laser and Sensor Applications. ACS Materials Letters. 2023; 5(4): 1261–1270. DOI: https://doi.org/10.1021/acsmaterialslett.2c01222.
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