PEMBUATAN ELEKTRODA PASTA KARBON UNTUK ANALISIS PARASETAMOL SECARA DIFFERENTIAL PULSE VOLTAMETRI

Authors

  • Firma Inggriani Universitas Negeri Surabaya
  • Pirim Setiarso Universitas Negeri Surabaya

Keywords:

Voltametri, Differential Pulse Voltametri, Pasta Karbon, Parasetamol

Abstract

In this study, carbon paste was made by carbon and paraffin for paracetamol detection by differential pulse voltametry. The main reason for using  carbon paste electrode for paracetamol detection is the conductive nature of carbon . Paracetamol detection of differential pulse voltammetric detection has several factors used to accurately detect paracetamol. Factors that can affect theelectrode composition, the pH of the solution, the deposition time, and the scan rate. In this study, paracetamol detection using carbon paste electrode has the optimum electrode composition in the ratio of Karbon with paraffin 8: 2. pH of optimum solution for detection of paracetamol 6, 5-second deposition time and scan rate 200 mV / sec. Pasta karbon electrode has  regresion 0.9889 with recovery 97.332% . the proposed sensor shows good selectivity, sensitivity, stable repetition and precision

Author Biography

Firma Inggriani, Universitas Negeri Surabaya

Department of Chemistry, State University of Surabaya

References

<p>1] Lima, Amanda B, et al., et al.   <em>Simultaneous determination of paracetamol and ibuprofen in pharmaceutical samples by differential pulse voltammetry using a boron-doped diamond electrode. </em>Brazil : Journal of Chemistry Society, 2014.</p><p>[2] May, Princess Rosdiana. <em>Relationship Knowledge and Parents Attitude Parents Behavior in Provision of Heat Lower Drugs (Antypretics) In Infant Age (0-1 year)Thesis . </em>Malang : Universitas Muhammadiyah Malang, 2012.</p><p>[3]  Wilson, John, et al., et al. <em>Analysis of acetaminophen metabolites in urine by high-performance liquid chromatography with UV andamperometric detection. </em>s.l. : Journal of Chromatography B: Biomedical Sciences and Applications, 1984. Vol 227. No 2.</p><p>[4] Curtius, H.C, et al., et al. <em>Mass fragmentography of dopamine and 6-hydroxydopamine: Application to the determination of dopamine in human brain biopsies from the caudate nucleus. . </em>s.l. : Journal of Chromatography , 2012.</p><p>[5] Maminski, Mariusz, et al., et al. <em>Spectrophotometric determination of dopamine in microliter scale using microfluidic system based on polymeric technology. . </em>s.l. : Analytica Chimica Acta, 2005. Vol. 540.No 1.</p><p>[6] Lukmana, Kuminingsih May. <em>Pembuatan Elektroda Kerja Graphene Oxide untuk Analisis Parasetamol secara Siklik Voltametri. </em>Surabaya : UNESA Journal of Chemistry, 2018. Vol.7 No.2.</p><p>[7] Suprasetyo, Amardi and Setiarso, Pirim. <em>PEMBUATAN ELEKTRODA PASTA KARBON TERMODIFIKASI ZEOLIT UNTUK ANALISIS FENOL SECARA CYCLIC STRIPPING VOLTAMMETRY. </em>Surabaya : UNESA Journal of Chemistry, 2016. VOl.5.No.3.</p><p>[8] Indra, Dyamarda. <em>Pembuatan Elektroda Kerja Graphene Oxide Untuk Analisis Fenol Secara Siklik Voltametri. </em>Surabaya : UNESA Journal of Chemistry, 2018.</p><p>1] Lima, Amanda B, et al., et al.   <em>Simultaneous determination of paracetamol and ibuprofen in pharmaceutical samples by differential pulse voltammetry using a boron-doped diamond electrode. </em>Brazil : Journal of Chemistry Society, 2014.</p><p>[2] May, Princess Rosdiana. <em>Relationship Knowledge and Parents Attitude Parents Behavior in Provision of Heat Lower Drugs (Antypretics) In Infant Age (0-1 year)Thesis . </em>Malang : Universitas Muhammadiyah Malang, 2012.</p><p>[3]  Wilson, John, et al., et al. <em>Analysis of acetaminophen metabolites in urine by high-performance liquid chromatography with UV andamperometric detection. </em>s.l. : Journal of Chromatography B: Biomedical Sciences and Applications, 1984. Vol 227. No 2.</p><p>[4] Curtius, H.C, et al., et al. <em>Mass fragmentography of dopamine and 6-hydroxydopamine: Application to the determination of dopamine in human brain biopsies from the caudate nucleus. . </em>s.l. : Journal of Chromatography , 2012.</p><p>[5] Maminski, Mariusz, et al., et al. <em>Spectrophotometric determination of dopamine in microliter scale using microfluidic system based on polymeric technology. . </em>s.l. : Analytica Chimica Acta, 2005. Vol. 540.No 1.</p><p>[6] Lukmana, Kuminingsih May. <em>Pembuatan Elektroda Kerja Graphene Oxide untuk Analisis Parasetamol secara Siklik Voltametri. </em>Surabaya : UNESA Journal of Chemistry, 2018. Vol.7 No.2.</p><p>[7] Suprasetyo, Amardi and Setiarso, Pirim. <em>PEMBUATAN ELEKTRODA PASTA KARBON TERMODIFIKASI ZEOLIT UNTUK ANALISIS FENOL SECARA CYCLIC STRIPPING VOLTAMMETRY. </em>Surabaya : UNESA Journal of Chemistry, 2016. VOl.5.No.3.</p><p>[8] Indra, Dyamarda. <em>Pembuatan Elektroda Kerja Graphene Oxide Untuk Analisis Fenol Secara Siklik Voltametri. </em>Surabaya : UNESA Journal of Chemistry, 2018.</p>

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Published

2022-01-10

Issue

Vol. 4 No. 2 (2021): Indonesian Chemistry and Application Journal

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